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TECHNIQUES- Etching
Sample Selection | Sectioning | Epoxy Mounting | Grinding & Polishing | Etching | Microscopy
The metal
microstructures can be revealed using
Nital (2 volume % HNO3,
balance ethanol), the standard etchant
for Fe-Ni alloys. Nital preferentially
reacts with kamacite (low-Ni) relative
to taenite (high Ni), and it also
enhances kamacite and taenite grain
boudaries. Optimal etching times
typically range from 30 to 60 seconds.
The etched specimen is washed with
ethanol and dried using a hair dryer.
It is
important to note that Nital will
release hydogen gas over time and can
become explosive. Therefore, it is
recommended that this etchant be
prepared and stored in small quantities. |